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. 2008 Mar 5;64(Pt 4):o656. doi: 10.1107/S160053680800562X
Oxford Diffraction Xcalibur S CCD diffractometer 2340 independent reflections
Radiation source: Enhance (Mo) X-ray source 2048 reflections with I > 2σ(I)
Monochromator: graphite Rint = 0.017
Detector resolution: 16.0696 pixels mm-1 θmax = 32.0º
T = 298(2) K θmin = 3.2º
ω and φ scans h = −8→8
Absorption correction: multi-scan(CrysAlis RED; Oxford Diffraction, 2006) k = −10→10
Tmin = 0.977, Tmax = 0.985 l = −14→14
64781 measured reflections