Oxford Diffraction Xcalibur S CCD diffractometer | 2340 independent reflections |
Radiation source: Enhance (Mo) X-ray source | 2048 reflections with I > 2σ(I) |
Monochromator: graphite | Rint = 0.017 |
Detector resolution: 16.0696 pixels mm-1 | θmax = 32.0º |
T = 298(2) K | θmin = 3.2º |
ω and φ scans | h = −8→8 |
Absorption correction: multi-scan(CrysAlis RED; Oxford Diffraction, 2006) | k = −10→10 |
Tmin = 0.977, Tmax = 0.985 | l = −14→14 |
64781 measured reflections |