| Enraf–Nonius CAD-4 diffractometer | Rint = 0.012 |
| Radiation source: fine-focus sealed tube | θmax = 30.0º |
| Monochromator: graphite | θmin = 1.9º |
| T = 293(2) K | h = 0→14 |
| θ/2θ scans | k = −16→14 |
| Absorption correction: none | l = −16→16 |
| 7089 measured reflections | 3 standard reflections |
| 6747 independent reflections | every 180 min |
| 4438 reflections with I > 2σ(I) | intensity decay: none |
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