Table 1. Hydrogen-bond geometry (Å, °).
D—H⋯A | D—H | H⋯A | D⋯A | D—H⋯A |
---|---|---|---|---|
N—HA⋯O3 | 0.89 | 1.96 | 2.8479 (14) | 174 |
N—HB⋯Cli | 0.89 | 2.31 | 3.1957 (11) | 171 |
N—HC⋯O3ii | 0.89 | 1.95 | 2.8380 (15) | 180 |
O2—H2⋯Cl | 0.82 | 2.23 | 3.0446 (11) | 175 |
O3—H4⋯Cliii | 0.82 (2) | 2.35 (2) | 3.1432 (12) | 161.0 (17) |
O3—H5⋯Cliv | 0.78 (2) | 2.38 (2) | 3.1283 (11) | 163.3 (16) |
Symmetry codes: (i) ; (ii) ; (iii) ; (iv) .