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. 2008 Apr 26;64(Pt 5):o922. doi: 10.1107/S1600536808011069
Bruker SMART APEXII diffractometer 1386 independent reflections
Radiation source: fine-focus sealed tube 1210 reflections with I > 2σ(I)
Monochromator: graphite Rint = 0.020
T = 100(2) K θmax = 27.5º
ω scans θmin = 1.5º
Absorption correction: multi-scan(SADABS; Sheldrick, 1996) h = −34→27
Tmin = 0.862, Tmax = 0.950 k = −5→5
3703 measured reflections l = −10→12