Bruker SMART APEXII diffractometer | 1386 independent reflections |
Radiation source: fine-focus sealed tube | 1210 reflections with I > 2σ(I) |
Monochromator: graphite | Rint = 0.020 |
T = 100(2) K | θmax = 27.5º |
ω scans | θmin = 1.5º |
Absorption correction: multi-scan(SADABS; Sheldrick, 1996) | h = −34→27 |
Tmin = 0.862, Tmax = 0.950 | k = −5→5 |
3703 measured reflections | l = −10→12 |