O1—C6 | 1.352 (3) | C9—H9B | 0.9700 |
O1—C9 | 1.441 (3) | C10—H10A | 0.9700 |
O2—C10 | 1.397 (3) | C10—H10B | 0.9700 |
O2—C11 | 1.419 (4) | C11—H11A | 0.9600 |
O3—C5 | 1.361 (3) | C11—H11B | 0.9600 |
O3—C12 | 1.436 (3) | C11—H11C | 0.9600 |
O4—C13 | 1.412 (3) | C12—C13 | 1.507 (3) |
O4—C14 | 1.412 (4) | C12—H12A | 0.9700 |
N1—C1 | 1.317 (3) | C12—H12B | 0.9700 |
N1—C8 | 1.378 (3) | C13—H13A | 0.9700 |
N1—HN1 | 0.8600 | C13—H13B | 0.9700 |
N2—C1 | 1.309 (3) | C14—H14A | 0.9600 |
N2—C2 | 1.353 (3) | C14—H14B | 0.9600 |
N3—C2 | 1.337 (3) | C14—H14C | 0.9600 |
N3—C15 | 1.427 (3) | C15—C16 | 1.388 (3) |
N3—H3 | 0.8600 | C15—C20 | 1.389 (3) |
C1—H1 | 0.9300 | C16—C17 | 1.382 (4) |
C2—C3 | 1.440 (3) | C16—H16 | 0.9300 |
C3—C8 | 1.400 (3) | C17—C18 | 1.375 (4) |
C3—C4 | 1.416 (3) | C17—H17 | 0.9300 |
C4—C5 | 1.368 (3) | C18—C19 | 1.386 (4) |
C4—H4 | 0.9300 | C18—H18 | 0.9300 |
C5—C6 | 1.429 (3) | C19—C20 | 1.399 (3) |
C6—C7 | 1.370 (3) | C19—C21 | 1.444 (4) |
C7—C8 | 1.397 (3) | C20—H20 | 0.9300 |
C7—H7 | 0.9300 | C21—C22 | 1.170 (4) |
C9—C10 | 1.491 (3) | C22—H22 | 0.95 (3) |
C9—H9A | 0.9700 | ||
C6—O1—C9 | 117.09 (19) | H10A—C10—H10B | 108.3 |
C10—O2—C11 | 111.7 (3) | O2—C11—H11A | 109.5 |
C5—O3—C12 | 116.48 (18) | O2—C11—H11B | 109.5 |
C13—O4—C14 | 112.8 (2) | H11A—C11—H11B | 109.5 |
C1—N1—C8 | 120.4 (2) | O2—C11—H11C | 109.5 |
C1—N1—HN1 | 119.8 | H11A—C11—H11C | 109.5 |
C8—N1—HN1 | 119.8 | H11B—C11—H11C | 109.5 |
C1—N2—C2 | 117.6 (2) | O3—C12—C13 | 106.5 (2) |
C2—N3—C15 | 127.4 (2) | O3—C12—H12A | 110.4 |
C2—N3—H3 | 116.3 | C13—C12—H12A | 110.4 |
C15—N3—H3 | 116.3 | O3—C12—H12B | 110.4 |
N2—C1—N1 | 125.4 (2) | C13—C12—H12B | 110.4 |
N2—C1—H1 | 117.3 | H12A—C12—H12B | 108.6 |
N1—C1—H1 | 117.3 | O4—C13—C12 | 111.1 (2) |
N3—C2—N2 | 117.4 (2) | O4—C13—H13A | 109.4 |
N3—C2—C3 | 121.2 (2) | C12—C13—H13A | 109.4 |
N2—C2—C3 | 121.4 (2) | O4—C13—H13B | 109.4 |
C8—C3—C4 | 117.6 (2) | C12—C13—H13B | 109.4 |
C8—C3—C2 | 116.7 (2) | H13A—C13—H13B | 108.0 |
C4—C3—C2 | 125.7 (2) | O4—C14—H14A | 109.5 |
C5—C4—C3 | 120.7 (2) | O4—C14—H14B | 109.5 |
C5—C4—H4 | 119.7 | H14A—C14—H14B | 109.5 |
C3—C4—H4 | 119.7 | O4—C14—H14C | 109.5 |
O3—C5—C4 | 125.2 (2) | H14A—C14—H14C | 109.5 |
O3—C5—C6 | 114.5 (2) | H14B—C14—H14C | 109.5 |
C4—C5—C6 | 120.3 (2) | C16—C15—C20 | 120.1 (2) |
O1—C6—C7 | 124.4 (2) | C16—C15—N3 | 117.1 (2) |
O1—C6—C5 | 115.7 (2) | C20—C15—N3 | 122.8 (2) |
C7—C6—C5 | 119.9 (2) | C17—C16—C15 | 119.7 (2) |
C6—C7—C8 | 119.2 (2) | C17—C16—H16 | 120.1 |
C6—C7—H7 | 120.4 | C15—C16—H16 | 120.1 |
C8—C7—H7 | 120.4 | C18—C17—C16 | 120.6 (3) |
N1—C8—C7 | 119.4 (2) | C18—C17—H17 | 119.7 |
N1—C8—C3 | 118.3 (2) | C16—C17—H17 | 119.7 |
C7—C8—C3 | 122.2 (2) | C17—C18—C19 | 120.2 (2) |
O1—C9—C10 | 108.1 (2) | C17—C18—H18 | 119.9 |
O1—C9—H9A | 110.1 | C19—C18—H18 | 119.9 |
C10—C9—H9A | 110.1 | C18—C19—C20 | 119.6 (2) |
O1—C9—H9B | 110.1 | C18—C19—C21 | 120.0 (2) |
C10—C9—H9B | 110.1 | C20—C19—C21 | 120.4 (2) |
H9A—C9—H9B | 108.4 | C15—C20—C19 | 119.6 (2) |
O2—C10—C9 | 108.7 (2) | C15—C20—H20 | 120.2 |
O2—C10—H10A | 109.9 | C19—C20—H20 | 120.2 |
C9—C10—H10A | 109.9 | C22—C21—C19 | 177.3 (3) |
O2—C10—H10B | 109.9 | C21—C22—H22 | 178 (2) |
C9—C10—H10B | 109.9 | ||
C2—N2—C1—N1 | 4.2 (4) | C1—N1—C8—C3 | −1.7 (4) |
C8—N1—C1—N2 | −2.7 (4) | C6—C7—C8—N1 | 177.9 (2) |
C15—N3—C2—N2 | 1.5 (4) | C6—C7—C8—C3 | −2.4 (4) |
C15—N3—C2—C3 | −178.7 (2) | C4—C3—C8—N1 | −177.0 (2) |
C1—N2—C2—N3 | 178.4 (2) | C2—C3—C8—N1 | 4.1 (3) |
C1—N2—C2—C3 | −1.3 (4) | C4—C3—C8—C7 | 3.4 (4) |
N3—C2—C3—C8 | 177.5 (2) | C2—C3—C8—C7 | −175.5 (2) |
N2—C2—C3—C8 | −2.7 (3) | C6—O1—C9—C10 | 176.3 (2) |
N3—C2—C3—C4 | −1.2 (4) | C11—O2—C10—C9 | −177.2 (3) |
N2—C2—C3—C4 | 178.5 (2) | O1—C9—C10—O2 | −76.9 (3) |
C8—C3—C4—C5 | −1.2 (3) | C5—O3—C12—C13 | −170.3 (2) |
C2—C3—C4—C5 | 177.5 (2) | C14—O4—C13—C12 | −79.6 (3) |
C12—O3—C5—C4 | −11.3 (3) | O3—C12—C13—O4 | −179.3 (2) |
C12—O3—C5—C6 | 168.7 (2) | C2—N3—C15—C16 | −146.2 (2) |
C3—C4—C5—O3 | 178.3 (2) | C2—N3—C15—C20 | 35.6 (4) |
C3—C4—C5—C6 | −1.7 (4) | C20—C15—C16—C17 | −1.7 (4) |
C9—O1—C6—C7 | −8.6 (3) | N3—C15—C16—C17 | −179.9 (2) |
C9—O1—C6—C5 | 172.4 (2) | C15—C16—C17—C18 | −0.1 (4) |
O3—C5—C6—O1 | 1.8 (3) | C16—C17—C18—C19 | 1.1 (4) |
C4—C5—C6—O1 | −178.3 (2) | C17—C18—C19—C20 | −0.5 (4) |
O3—C5—C6—C7 | −177.3 (2) | C17—C18—C19—C21 | 179.5 (3) |
C4—C5—C6—C7 | 2.7 (4) | C16—C15—C20—C19 | 2.4 (4) |
O1—C6—C7—C8 | −179.6 (2) | N3—C15—C20—C19 | −179.6 (2) |
C5—C6—C7—C8 | −0.6 (4) | C18—C19—C20—C15 | −1.3 (4) |
C1—N1—C8—C7 | 177.9 (2) | C21—C19—C20—C15 | 178.7 (2) |