Bruker APEX area-detector diffractometer	3649 reflections with I > 2σ(I)
Radiation source: fine-focus sealed tube	Rint = 0.050
Monochromator: graphite	θmax = 28.0º
T = 293(2) K	θmin = 1.8º
ω scans	h = −18→19
Absorption correction: none	k = −24→24
24377 measured reflections	l = −10→10
5001 independent reflections