| Bruker SMART CCD area-detector diffractometer | 2437 independent reflections |
| Radiation source: fine-focus sealed tube | 1543 reflections with I > 2σ(I) |
| Monochromator: graphite | Rint = 0.030 |
| T = 291(2) K | θmax = 25.5º |
| φ and ω scans | θmin = 2.5º |
| Absorption correction: multi-scan(SADABS; Sheldrick, 1996) | h = −10→10 |
| Tmin = 0.969, Tmax = 0.991 | k = −15→15 |
| 9588 measured reflections | l = −15→15 |