| Oxford Diffraction XCALIBUR diffractometer | 1750 independent reflections |
| Radiation source: Enhance (Mo) X-ray Source | 1144 reflections with I > 2σ(I) |
| Monochromator: graphite | Rint = 0.018 |
| Detector resolution: 16.0143 pixels mm-1 | θmax = 32.7º |
| T = 175 K | θmin = 3.9º |
| ω scans | h = −5→6 |
| Absorption correction: multi-scan(CrysAlis RED; Oxford Diffraction, 2007); empirical (using intensity measurements) absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm | k = −31→29 |
| Tmin = 0.95, Tmax = 0.97 | l = −17→15 |
| 7752 measured reflections |