Bruker SMART 1000 CCD diffractometer | 3713 independent reflections |
Radiation source: fine-focus sealed tube | 3026 reflections with I > 2σ(I) |
Monochromator: graphite | Rint = 0.042 |
T = 173(2) K | θmax = 27.0º |
ω scans | θmin = 1.9º |
Absorption correction: multi-scan(SADABS; Sheldrick, 2003) | h = −16→15 |
Tmin = 0.954, Tmax = 0.988 | k = −16→19 |
18319 measured reflections | l = −16→19 |