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. 2008 May 10;64(Pt 6):o1033–o1034. doi: 10.1107/S1600536808013147
Bruker SMART 1000 CCD diffractometer 3713 independent reflections
Radiation source: fine-focus sealed tube 3026 reflections with I > 2σ(I)
Monochromator: graphite Rint = 0.042
T = 173(2) K θmax = 27.0º
ω scans θmin = 1.9º
Absorption correction: multi-scan(SADABS; Sheldrick, 2003) h = −16→15
Tmin = 0.954, Tmax = 0.988 k = −16→19
18319 measured reflections l = −16→19