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. 2008 May 10;64(Pt 6):o1025. doi: 10.1107/S1600536808012154
Bruker SMART APEX CCD diffractometer 2307 independent reflections
Radiation source: fine-focus sealed tube 2054 reflections with I > 2σ(I)
Monochromator: graphite Rint = 0.038
T = 293(2) K θmax = 27.0º
φ and ω scans θmin = 2.1º
Absorption correction: multi-scan(SADABS; Sheldrick, 1996) h = −7→7
Tmin = 0.381, Tmax = 1.000 k = −12→15
4117 measured reflections l = −12→12