Bruker SMART APEX CCD diffractometer | 2307 independent reflections |
Radiation source: fine-focus sealed tube | 2054 reflections with I > 2σ(I) |
Monochromator: graphite | Rint = 0.038 |
T = 293(2) K | θmax = 27.0º |
φ and ω scans | θmin = 2.1º |
Absorption correction: multi-scan(SADABS; Sheldrick, 1996) | h = −7→7 |
Tmin = 0.381, Tmax = 1.000 | k = −12→15 |
4117 measured reflections | l = −12→12 |