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. 2008 May 3;64(Pt 6):o950. doi: 10.1107/S1600536808012385
Oxford Diffraction Xcalibur diffractometer 2311 independent reflections
Monochromator: graphite 1209 reflections with I > 2σ(I)
Detector resolution: 10.434 pixels mm-1 Rint = 0.060
T = 295(2) K θmax = 25.7º
ω scans with κ offsets θmin = 5.1º
Absorption correction: analytical[CrysAlis RED (Oxford Diffraction, 2007), based on expressions derived by Clark & Reid (1995)] h = −14→14
Tmin = 0.905, Tmax = 0.987 k = −5→5
11465 measured reflections l = −27→27