Oxford Diffraction Xcalibur diffractometer | 2311 independent reflections |
Monochromator: graphite | 1209 reflections with I > 2σ(I) |
Detector resolution: 10.434 pixels mm-1 | Rint = 0.060 |
T = 295(2) K | θmax = 25.7º |
ω scans with κ offsets | θmin = 5.1º |
Absorption correction: analytical[CrysAlis RED (Oxford Diffraction, 2007), based on expressions derived by Clark & Reid (1995)] | h = −14→14 |
Tmin = 0.905, Tmax = 0.987 | k = −5→5 |
11465 measured reflections | l = −27→27 |