| Bruker SMART APEX CCD area-detector diffractometer | 2276 independent reflections |
| Monochromator: parallel mounted graphite | 1848 reflections with I > 2σ(I) |
| Detector resolution: 66.06 pixels mm-1 | Rint = 0.028 |
| T = 100(1) K | θmax = 26.0º |
| φ and ω scans | θmin = 3.0º |
| Absorption correction: multi-scan(SADABS; Bruker, 2007) | h = −9→9 |
| Tmin = 0.956, Tmax = 0.982 | k = −16→15 |
| 8700 measured reflections | l = −14→14 |
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