| Bruker SMART CCD area-detector diffractometer | 2119 independent reflections |
| Radiation source: fine-focus sealed tube | 1460 reflections with I > 2σ(I) |
| Monochromator: graphite | Rint = 0.051 |
| T = 296(2) K | θmax = 26.5º |
| φ and ω scans | θmin = 2.6º |
| Absorption correction: multi-scan(SADABS; Sheldrick, 1996) | h = −9→9 |
| Tmin = 0.921, Tmax = 0.987 | k = −17→15 |
| 11412 measured reflections | l = −11→12 |