Bruker SMART APEXII CCD area-detector diffractometer	5431 independent reflections
Radiation source: fine-focus sealed tube	4559 reflections with I > 2σ(I)
Monochromator: graphite	Rint = 0.045
Detector resolution: 8.33 pixels mm-1	θmax = 30.1º
T = 100.0(1) K	θmin = 2.5º
ω scans	h = −17→23
Absorption correction: multi-scan(SADABS; Bruker, 2005)	k = −9→9
Tmin = 0.952, Tmax = 0.979	l = −43→44
37248 measured reflections