| Refinement on F2 | Primary atom site location: structure-invariant direct methods |
| Least-squares matrix: full | Hydrogen site location: inferred from neighbouring sites |
| R[F2 > 2σ(F2)] = 0.080 | H-atom parameters not refined |
| wR(F2) = 0.178 | Method = Modified Sheldrick w = 1/[σ2(F2) + ( 0.06P)2 + 0.42P] ,where P = (max(Fo2,0) + 2Fc2)/3 |
| S = 1.05 | (Δ/σ)max = 0.0004 |
| 2984 reflections | Δρmax = 0.73 e Å−3 |
| 236 parameters | Δρmin = −0.60 e Å−3 |
| 24 restraints | Extinction correction: None |