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. 2008 Jun 7;64(Pt 7):o1215–o1216. doi: 10.1107/S1600536808016577
Refinement on F2 Primary atom site location: structure-invariant direct methods
Least-squares matrix: full Hydrogen site location: inferred from neighbouring sites
R[F2 > 2σ(F2)] = 0.080 H-atom parameters not refined
wR(F2) = 0.178   Method = Modified Sheldrick w = 1/[σ2(F2) + ( 0.06P)2 + 0.42P] ,where P = (max(Fo2,0) + 2Fc2)/3
S = 1.05 (Δ/σ)max = 0.0004
2984 reflections Δρmax = 0.73 e Å3
236 parameters Δρmin = −0.60 e Å3
24 restraints Extinction correction: None