| Oxford Diffraction Xcalibur diffractometer | 2686 independent reflections |
| Radiation source: fine-focus sealed tube | 1288 reflections with I > 2σ(I) |
| Monochromator: graphite | Rint = 0.094 |
| T = 299(2) K | θmax = 26.4º |
| Rotation method using ω and φ scans | θmin = 2.4º |
| Absorption correction: multi-scan(CrysAlis RED; Oxford Diffraction, 2007) | h = −16→18 |
| Tmin = 0.781, Tmax = 0.960 | k = −10→10 |
| 12954 measured reflections | l = −25→25 |