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. 2008 Jun 19;64(Pt 7):o1294. doi: 10.1107/S1600536808018072
Oxford Diffraction Xcalibur diffractometer 2686 independent reflections
Radiation source: fine-focus sealed tube 1288 reflections with I > 2σ(I)
Monochromator: graphite Rint = 0.094
T = 299(2) K θmax = 26.4º
Rotation method using ω and φ scans θmin = 2.4º
Absorption correction: multi-scan(CrysAlis RED; Oxford Diffraction, 2007) h = −16→18
Tmin = 0.781, Tmax = 0.960 k = −10→10
12954 measured reflections l = −25→25