Bruker APEXII CCD area-detector diffractometer | 6379 independent reflections |
Radiation source: fine-focus sealed tube | 6016 reflections with I > 2σ(I) |
Monochromator: graphite | Rint = 0.035 |
T = 100(2) K | θmax = 30.0º |
ω scans | θmin = 2.0º |
Absorption correction: multi-scan(SADABS; Sheldrick, 1996) | h = −29→29 |
Tmin = 0.781, Tmax = 0.898 | k = −11→11 |
36654 measured reflections | l = −17→17 |