| Bruker SMART APEXII CCD area-detector diffractometer | 6478 independent reflections |
| Radiation source: fine-focus sealed tube | 4651 reflections with I > 2σ(I)) |
| Monochromator: graphite | Rint = 0.035 |
| T = 100.0(1) K | θmax = 29.3º |
| φ and ω scans | θmin = 2.3º |
| Absorption correction: multi-scan(SADABS; Bruker, 2005) | h = −12→11 |
| Tmin = 0.955, Tmax = 0.985 | k = −12→12 |
| 26162 measured reflections | l = −20→20 |