Bruker P4 diffractometer | Rint = 0.019 |
Radiation source: fine-focus sealed tube | θmax = 27.5º |
Monochromator: graphite | θmin = 3.3º |
T = 295(2) K | h = −13→13 |
θ/2θ scans | k = −10→9 |
Absorption correction: multi-scan(XSCANS; Siemens, 1996) | l = −24→25 |
Tmin = 0.749, Tmax = 0.879 | 3 standard reflections |
15099 measured reflections | every 97 reflections |
3632 independent reflections | intensity decay: none |
3202 reflections with I > 2σ(I) |