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. 2008 Jul 26;64(Pt 8):m1062. doi: 10.1107/S1600536808022812
Bruker P4 diffractometer Rint = 0.019
Radiation source: fine-focus sealed tube θmax = 27.5º
Monochromator: graphite θmin = 3.3º
T = 295(2) K h = −13→13
θ/2θ scans k = −10→9
Absorption correction: multi-scan(XSCANS; Siemens, 1996) l = −24→25
Tmin = 0.749, Tmax = 0.879 3 standard reflections
15099 measured reflections every 97 reflections
3632 independent reflections intensity decay: none
3202 reflections with I > 2σ(I)