| Bruker SMART APEX diffractometer | 3125 independent reflections |
| Radiation source: fine-focus sealed tube | 2491 reflections with I > 2σ(I) |
| Monochromator: graphite | Rint = 0.024 |
| T = 295(2) K | θmax = 27.5º |
| φ and ω scans | θmin = 2.5º |
| Absorption correction: multi-scan(SADABS; Sheldrick, 1996) | h = −13→13 |
| Tmin = 0.540, Tmax = 0.705 | k = −16→15 |
| 8685 measured reflections | l = −16→27 |
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