| Bruker SMART ApexII CCD diffractometer | 19555 independent reflections |
| Radiation source: fine-focus sealed tube | 16163 reflections with I > 2σ(I) |
| Monochromator: graphite | Rint = 0.040 |
| T = 291(2) K | θmax = 25.5º |
| phi and ω scans | θmin = 1.2º |
| Absorption correction: multi-scan(SADABS; Bruker, 2000) | h = −18→18 |
| Tmin = 0.375, Tmax = 0.435 | k = −21→21 |
| 63226 measured reflections | l = −24→21 |
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