| Bruker SMART APEXII CCD area-detector diffractometer | 5156 independent reflections |
| Radiation source: fine-focus sealed tube | 4138 reflections with I > 2σ(I) |
| Monochromator: graphite | Rint = 0.028 |
| T = 100.0(1) K | θmax = 35.0º |
| φ and ω scans | θmin = 3.1º |
| Absorption correction: multi-scan(SADABS; Bruker, 2005) | h = −21→19 |
| Tmin = 0.939, Tmax = 0.977 | k = −10→12 |
| 22302 measured reflections | l = −20→20 |