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. 2008 Jul 12;64(Pt 8):o1466. doi: 10.1107/S1600536808020953
Bruker SMART APEXII CCD area-detector diffractometer 5156 independent reflections
Radiation source: fine-focus sealed tube 4138 reflections with I > 2σ(I)
Monochromator: graphite Rint = 0.028
T = 100.0(1) K θmax = 35.0º
φ and ω scans θmin = 3.1º
Absorption correction: multi-scan(SADABS; Bruker, 2005) h = −21→19
Tmin = 0.939, Tmax = 0.977 k = −10→12
22302 measured reflections l = −20→20