Bruker SMART CCD area-detector diffractometer | 3627 independent reflections |
Radiation source: fine-focus sealed tube | 1895 reflections with I > 2σ(I) |
Monochromator: graphite | Rint = 0.101 |
T = 298(2) K | θmax = 27.0º |
ω scans | θmin = 2.1º |
Absorption correction: multi-scan(SADABS; Sheldrick, 1996) | h = −14→14 |
Tmin = 0.402, Tmax = 0.444 | k = −12→10 |
9035 measured reflections | l = −23→22 |