Nonius KappaCCD area-detector diffractometer | 2801 reflections with I > 2σ(I) |
Radiation source: fine-focus sealed tube | Rint = 0.059 |
Monochromator: graphite | θmax = 28.5º |
φ scans, and ω scans with κ offsets | θmin = 1.4º |
Absorption correction: multi-scan(SORTAV; Blessing, 1995) | h = −31→37 |
Tmin = 0.380, Tmax = 0.600 | k = −36→35 |
11358 measured reflections | l = −7→11 |
3251 independent reflections |