Refinement on F2 | H-atom parameters constrained |
Least-squares matrix: full | w = 1/[σ2(Fo2) + (0.087P)2 + 39.1076P] where P = (Fo2 + 2Fc2)/3 |
R[F2 > 2σ(F2)] = 0.072 | (Δ/σ)max = 0.001 |
wR(F2) = 0.205 | Δρmax = 1.04 e Å−3 |
S = 1.21 | Δρmin = −1.05 e Å−3 |
3251 reflections | Extinction correction: SHELXL97 (Sheldrick, 2008), Fc*=kFc[1+0.001xFc2λ3/sin(2θ)]-1/4 |
166 parameters | Extinction coefficient: 0.0064 (7) |