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. 2008 Jul 5;64(Pt 8):o1387. doi: 10.1107/S1600536808019491
Refinement on F2 H-atom parameters constrained
Least-squares matrix: full   w = 1/[σ2(Fo2) + (0.087P)2 + 39.1076P] where P = (Fo2 + 2Fc2)/3
R[F2 > 2σ(F2)] = 0.072 (Δ/σ)max = 0.001
wR(F2) = 0.205 Δρmax = 1.04 e Å3
S = 1.21 Δρmin = −1.05 e Å3
3251 reflections Extinction correction: SHELXL97 (Sheldrick, 2008), Fc*=kFc[1+0.001xFc2λ3/sin(2θ)]-1/4
166 parameters Extinction coefficient: 0.0064 (7)