| Bruker APEXII CCD area-detector diffractometer | 1791 independent reflections |
| Radiation source: fine-focus sealed tube | 1118 reflections with I > 2σ(I) |
| Monochromator: graphite | Rint = 0.066 |
| Detector resolution: 7.40 pixels mm-1 | θmax = 29.2º |
| T = 296(2) K | θmin = 2.4º |
| φ and ω scans | h = −20→23 |
| Absorption correction: none | k = −23→24 |
| 8129 measured reflections | l = −11→7 |
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