| Enraf–Nonius CAD-4 diffractometer | Rint = 0.018 |
| Radiation source: fine-focus sealed tube | θmax = 25.5º |
| Monochromator: graphite | θmin = 1.2º |
| T = 291(2) K | h = −6→24 |
| ω/2θ scans | k = −13→0 |
| Absorption correction: none | l = −20→20 |
| 4309 measured reflections | 3 standard reflections |
| 3705 independent reflections | every 300 reflections |
| 2282 reflections with I > 2σ(I) | intensity decay: 2.6% |
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