| Bruker SMART CCD area-detector diffractometer | 1764 independent reflections |
| Radiation source: fine-focus sealed tube | 1438 reflections with I > 2σ(I) |
| Monochromator: graphite | Rint = 0.065 |
| T = 298(2) K | θmax = 25.0º |
| φ and ω scans | θmin = 1.9º |
| Absorption correction: multi-scan(SADABS; Sheldrick, 1996) | h = −7→7 |
| Tmin = 0.871, Tmax = 0.924 | k = −9→6 |
| 4749 measured reflections | l = −25→24 |