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. 2008 Jul 9;64(Pt 8):o1451. doi: 10.1107/S1600536808019430
Bruker SMART CCD APEXII diffractometer 4284 independent reflections
Radiation source: fine-focus sealed tube 2948 reflections with I > 2σ(I)
Monochromator: graphite Rint = 0.029
Detector resolution: 8.40 pixels mm-1 θmax = 27.5º
T = 298(2) K θmin = 3.1º
ω scans h = −8→7
Absorption correction: multi-scan(SADABS; Sheldrick, 1996) k = −14→14
Tmin = 0.968, Tmax = 0.977 l = −17→17
9385 measured reflections