| Bruker SMART CCD APEXII diffractometer | 4284 independent reflections |
| Radiation source: fine-focus sealed tube | 2948 reflections with I > 2σ(I) |
| Monochromator: graphite | Rint = 0.029 |
| Detector resolution: 8.40 pixels mm-1 | θmax = 27.5º |
| T = 298(2) K | θmin = 3.1º |
| ω scans | h = −8→7 |
| Absorption correction: multi-scan(SADABS; Sheldrick, 1996) | k = −14→14 |
| Tmin = 0.968, Tmax = 0.977 | l = −17→17 |
| 9385 measured reflections |