Rigaku Saturn CCD area-detector diffractometer | 2581 independent reflections |
Radiation source: rotating anode | 2449 reflections with I > 2σ(I) |
Monochromator: confocal | Rint = 0.037 |
Detector resolution: 7.31 pixels mm-1 | θmax = 27.8º |
T = 113(2) K | θmin = 2.1º |
ω scans | h = −12→12 |
Absorption correction: multi-scan(CrystalClear; Rigaku/MSC, 2005) | k = −11→13 |
Tmin = 0.987, Tmax = 0.991 | l = −26→16 |
13910 measured reflections |