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. 2008 Jul 19;64(Pt 8):o1538. doi: 10.1107/S1600536808021752
Rigaku Saturn CCD area-detector diffractometer 2581 independent reflections
Radiation source: rotating anode 2449 reflections with I > 2σ(I)
Monochromator: confocal Rint = 0.037
Detector resolution: 7.31 pixels mm-1 θmax = 27.8º
T = 113(2) K θmin = 2.1º
ω scans h = −12→12
Absorption correction: multi-scan(CrystalClear; Rigaku/MSC, 2005) k = −11→13
Tmin = 0.987, Tmax = 0.991 l = −26→16
13910 measured reflections