Refinement on F2
|
Secondary atom site location: difference Fourier map |
Least-squares matrix: full |
Hydrogen site location: inferred from neighbouring sites |
R[F2 > 2σ(F2)] = 0.064 |
H atoms treated by a mixture of independent and constrained refinement |
wR(F2) = 0.155 |
w = 1/[σ2(Fo2) + (0.0499P)2 + 10.2476P] where P = (Fo2 + 2Fc2)/3 |
S = 1.22 |
(Δ/σ)max = 0.001 |
3424 reflections |
Δρmax = 1.08 e Å−3
|
241 parameters |
Δρmin = −1.82 e Å−3
|
10 restraints |
Extinction correction: none |
Primary atom site location: structure-invariant direct methods |
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