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. Author manuscript; available in PMC: 2011 Nov 2.
Published in final edited form as: Biochemistry. 2010 Nov 2;49(43):9306–9317. doi: 10.1021/bi101336u

Table 1.

Crystallographic Data Collection Statistics

Dataset Native 1 Native 2
Resolution (Å)a 50.0-3.60 (3.73-3.60) 50-3.15 (3.26-3.15)
Space group P65 P65
Unit cell dimensions (Ǻ) a=b=104.01 c=294.36 a=b=103.81 c=295.95
Rsymb 6.3 (43.8) 11.6 (47.4)
Completeness (%) 99.8 (100.0) 99.6 (99.5)
Imean/σ 29.2 (5.4) 8.93 (2.50)
# total reflections 159943 127962
# unique reflections 20697 (2046) 31158 (3113)
Redundancy 7.7 (7.7) 4.1 (3.5)
wavelength (Å) 1.12713 1.20000
Beamline APS 21-ID-D APS 21-ID-D
a

Values in parenthesis refer to the high-resolution bin.

b

Rsym = Σhkl Σi |Ii(hkl) - I(hkl)| (100) / ΣhklΣi Ii(hkl), where Ii(hkl) and I(hkl) are the ith and mean measurements of the intensity of reflection hkl.