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. Author manuscript; available in PMC: 2010 Oct 27.
Published in final edited form as: Tetrahedron. 2009 Aug 29;65(35):7277–7288. doi: 10.1016/j.tet.2009.01.110

Figure 7.

Figure 7

Selected regions of the 1H NMR spectra (500 MHz, D2O, 5 × 10-3 M OA and 5 × 10-2 M sodium tetraborate) showing the aliphatic regions of OA complexes of 1a, 1b, 1c, 1d and 1e. Methyl groups of the chiral auxiliary and of the pyridone ring are labeled 1 and 2 respectively as shown in each figure. Change in chemical shift upon binding to OA with respect to the NMR spectrum recorded in CDCl3 (Δδ) is also shown for each signal.