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. Author manuscript; available in PMC: 2010 Oct 30.
Published in final edited form as: J Am Chem Soc. 2005 Mar 9;127(9):2866–2867. doi: 10.1021/ja0425583

Table 6.

One-Pot Enantioselective Synthesis of Branched Allylic Esters

graphic file with name nihms245298t8.jpg
entry R temp
[°C]
4 yield
[%]a
ee
[%]
1 Me 23 4c 76 92b
2 Ph 38 4i 72 80c
3 p-MeOC6H4 38 4m 94 90c
4 graphic file with name nihms245298t9.jpg 38 4v 64 87d
a

Yield of pure product after silica gel chromatography.

b

Determined by GC analysis.

c

Determined by SFC analysis.

d

Determined by HPLC analysis.