| Rigaku Mercury CCD diffractometer | 4449 independent reflections |
| Radiation source: Sealed Tube | 3288 reflections with I > 2σ(I) |
| Graphite Monochromator | Rint = 0.089 |
| Detector resolution: 14.6306 pixels mm-1 | θmax = 25.0°, θmin = 2.3° |
| ω scans | h = −9→9 |
| Absorption correction: multi-scan (REQAB; Jacobson, 1998) | k = −30→33 |
| Tmin = 0.581, Tmax = 0.955 | l = −14→14 |
| 17799 measured reflections |
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