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. 2008 Dec 10;65(Pt 1):o64. doi: 10.1107/S1600536808040993
Oxford Diffraction Gemini R diffractometer 4842 independent reflections
Radiation source: fine-focus sealed tube 2832 reflections with I > 2σ(I)
graphite Rint = 0.035
Detector resolution: 10.5081 pixels mm-1 θmax = 32.6°, θmin = 4.6°
φ and ω scans h = −8→8
Absorption correction: multi-scan (CrysAlis RED; Oxford Diffraction, 2007) k = −12→12
Tmin = 0.887, Tmax = 1.000 l = −44→44
13882 measured reflections