Oxford Diffraction Gemini R diffractometer | 4842 independent reflections |
Radiation source: fine-focus sealed tube | 2832 reflections with I > 2σ(I) |
graphite | Rint = 0.035 |
Detector resolution: 10.5081 pixels mm-1 | θmax = 32.6°, θmin = 4.6° |
φ and ω scans | h = −8→8 |
Absorption correction: multi-scan (CrysAlis RED; Oxford Diffraction, 2007) | k = −12→12 |
Tmin = 0.887, Tmax = 1.000 | l = −44→44 |
13882 measured reflections |