| Bruker SMART APEX diffractometer | 3942 independent reflections |
| Radiation source: fine-focus sealed tube | 3605 reflections with I > 2σ(I) |
| graphite | Rint = 0.013 |
| ω scans | θmax = 27.5°, θmin = 1.4° |
| Absorption correction: multi-scan (SADABS; Sheldrick, 1996) | h = −6→8 |
| Tmin = 0.807, Tmax = 1.000 | k = −12→12 |
| 6268 measured reflections | l = −19→19 |