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. 2008 Dec 13;65(Pt 1):o121–o122. doi: 10.1107/S1600536808042086
Rigaku AFC-8S Mercury CCD diffractometer 4010 independent reflections
Radiation source: Sealed Tube 3051 reflections with I > 2σ(I)
Graphite Monochromator Rint = 0.060
Detector resolution: 14.6199 pixels mm-1 θmax = 25.1°, θmin = 2.2°
ω scans h = −22→22
Absorption correction: multi-scan (REQAB; Jacobson, 1998) k = −16→16
Tmin = 0.615, Tmax = 0.798 l = −10→10
18802 measured reflections