Rigaku AFC-8S Mercury CCD diffractometer | 4010 independent reflections |
Radiation source: Sealed Tube | 3051 reflections with I > 2σ(I) |
Graphite Monochromator | Rint = 0.060 |
Detector resolution: 14.6199 pixels mm-1 | θmax = 25.1°, θmin = 2.2° |
ω scans | h = −22→22 |
Absorption correction: multi-scan (REQAB; Jacobson, 1998) | k = −16→16 |
Tmin = 0.615, Tmax = 0.798 | l = −10→10 |
18802 measured reflections |