| Bruker SMART APEX CCD diffractometer | 1772 independent reflections |
| Radiation source: fine-focus sealed tube | 1519 reflections with I > 2σ(I) |
| graphite | Rint = 0.026 |
| φ and ω scans | θmax = 27.5°, θmin = 3.0° |
| Absorption correction: multi-scan (SADABS; Sheldrick, 2001) | h = −9→9 |
| Tmin = 0.967, Tmax = 0.989 | k = −8→10 |
| 5336 measured reflections | l = −14→17 |
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