| Bruker SMART APEXII detector diffractometer | 1550 independent reflections |
| Radiation source: fine-focus sealed tube | 1273 reflections with I > 2σ(I) |
| graphite | Rint = 0.022 |
| phi and ω scans | θmax = 25.5°, θmin = 3.0° |
| Absorption correction: multi-scan (SADABS; Sheldrick, 1996) | h = −12→12 |
| Tmin = 0.961, Tmax = 0.976 | k = −15→15 |
| 11505 measured reflections | l = −15→15 |