| Rigaku R-AXIS RAPID diffractometer | 2559 reflections with F2 > 2σ(F2) |
| Detector resolution: 10.00 pixels mm-1 | Rint = 0.027 |
| ω scans | θmax = 27.4° |
| Absorption correction: multi-scan (ABSCOR; Higashi, 1995) | h = −19→19 |
| Tmin = 0.858, Tmax = 0.911 | k = −22→22 |
| 15655 measured reflections | l = −16→15 |
| 3708 independent reflections |