| Bruker Kappa APEXII CCD diffractometer | 3885 independent reflections |
| Radiation source: fine-focus sealed tube | 2825 reflections with I > 2σ(I) |
| graphite | Rint = 0.028 |
| ω and φ scan | θmax = 27.0°, θmin = 2.2° |
| Absorption correction: multi-scan (SADABS; Bruker, 2004) | h = −9→10 |
| Tmin = 0.945, Tmax = 0.956 | k = −14→14 |
| 17066 measured reflections | l = −14→14 |