| Bruker SMART CCD area-detector diffractometer | 4774 independent reflections |
| Radiation source: fine-focus sealed tube | 3201 reflections with I > 2σ(I) |
| graphite | Rint = 0.041 |
| φ and ω scans | θmax = 25.0°, θmin = 1.8° |
| Absorption correction: multi-scan (SADABS; Bruker, 1999) | h = −12→11 |
| Tmin = 0.915, Tmax = 0.954 | k = −13→13 |
| 11871 measured reflections | l = −23→26 |