Mercury CCD diffractometer | 4860 independent reflections |
Radiation source: Sealed Tube | 3921 reflections with I > 2σ(I) |
Graphite Monochromator | Rint = 0.022 |
Detector resolution: 14.6306 pixels mm-1 | θmax = 25.0°, θmin = 3.2° |
ω scans | h = −12→12 |
Absorption correction: multi-scan (REQAB; Jacobson, 1998) | k = −12→12 |
Tmin = 0.514, Tmax = 0.673 | l = −16→16 |
11938 measured reflections |