| Bruker APEXII CCD diffractometer | 8753 reflections with I > 2σ(I) |
| Radiation source: fine-focus sealed tube | Rint = 0.050 |
| ω and φ scans | θmax = 26.4°, θmin = 1.6° |
| Absorption correction: multi-scan (SADABS; Bruker, 2005) | h = −15→15 |
| Tmin = 0.575, Tmax = 0.830 | k = −16→16 |
| 49577 measured reflections | l = 0→21 |
| 11468 independent reflections |
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