Bruker X8 APEXII diffractometer | 2592 independent reflections |
Radiation source: fine-focus sealed tube | 1097 reflections with I > 2σ(I) |
graphite | Rint = 0.082 |
φ and ω scans | θmax = 25.0°, θmin = 2.5° |
Absorption correction: multi-scan (SADABS; Bruker, 2008) | h = −4→4 |
Tmin = 0.591, Tmax = 0.914 | k = −16→16 |
4633 measured reflections | l = −19→19 |