| Rigaku Mercury CCD diffractometer | 3914 reflections with I > 2σ(I) |
| Radiation source: Rotating Anode | Rint = 0.024 |
| Graphite Monochromator | θmax = 27.5°, θmin = 3.1° |
| Detector resolution: 14.7059 pixels mm-1 | h = −11→10 |
| φ and ω scans | k = −22→25 |
| 15238 measured reflections | l = −15→12 |
| 4638 independent reflections |
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