Ni1—N3 | 2.0344 (18) | C10—H10 | 0.9300 |
Ni1—N1 | 2.0418 (18) | C11—C12 | 1.384 (3) |
Ni1—N4 | 2.0879 (17) | C11—H11 | 0.9300 |
Ni1—N2 | 2.1188 (17) | C12—H12 | 0.9300 |
Ni1—Cl1 | 2.3944 (6) | C13—C14 | 1.379 (3) |
Ni1—Cl2 | 2.4153 (7) | C13—H13 | 0.9300 |
O1—N1 | 1.373 (2) | C14—C15 | 1.370 (3) |
O1—H1 | 0.8200 | C14—H14 | 0.9300 |
O2—N3 | 1.383 (2) | C15—C16 | 1.381 (3) |
O2—H2 | 0.8200 | C15—H15 | 0.9300 |
O3—C26 | 1.200 (3) | C16—C17 | 1.382 (3) |
N1—C6 | 1.290 (3) | C16—H16 | 0.9300 |
N2—C1 | 1.328 (3) | C17—C18 | 1.486 (3) |
N2—C5 | 1.352 (3) | C18—C19 | 1.477 (3) |
N3—C18 | 1.292 (3) | C19—C20 | 1.386 (3) |
N4—C13 | 1.335 (3) | C19—C24 | 1.393 (3) |
N4—C17 | 1.356 (3) | C20—C21 | 1.386 (3) |
C1—C2 | 1.389 (3) | C20—H20 | 0.9300 |
C1—H1A | 0.9300 | C21—C22 | 1.371 (4) |
C2—C3 | 1.363 (4) | C21—H21 | 0.9300 |
C2—H2A | 0.9300 | C22—C23 | 1.367 (4) |
C3—C4 | 1.381 (4) | C22—H22 | 0.9300 |
C3—H3 | 0.9300 | C23—C24 | 1.386 (3) |
C4—C5 | 1.392 (3) | C23—H23 | 0.9300 |
C4—H4 | 0.9300 | C24—H24 | 0.9300 |
C5—C6 | 1.488 (3) | C25—C26 | 1.464 (5) |
C6—C7 | 1.477 (3) | C25—H25A | 0.9600 |
C7—C12 | 1.387 (3) | C25—H25B | 0.9600 |
C7—C8 | 1.392 (3) | C25—H25C | 0.9600 |
C8—C9 | 1.380 (4) | C26—C27 | 1.477 (4) |
C8—H8 | 0.9300 | C27—H27A | 0.9600 |
C9—C10 | 1.382 (4) | C27—H27B | 0.9600 |
C9—H9 | 0.9300 | C27—H27C | 0.9600 |
C10—C11 | 1.365 (4) | ||
N3—Ni1—N1 | 170.18 (7) | C9—C10—H10 | 120.1 |
N3—Ni1—N4 | 76.84 (7) | C10—C11—C12 | 120.4 (3) |
N1—Ni1—N4 | 99.25 (7) | C10—C11—H11 | 119.8 |
N3—Ni1—N2 | 94.03 (7) | C12—C11—H11 | 119.8 |
N1—Ni1—N2 | 76.92 (7) | C11—C12—C7 | 120.3 (2) |
N4—Ni1—N2 | 91.16 (7) | C11—C12—H12 | 119.9 |
N3—Ni1—Cl1 | 99.43 (5) | C7—C12—H12 | 119.9 |
N1—Ni1—Cl1 | 89.47 (5) | N4—C13—C14 | 122.8 (2) |
N4—Ni1—Cl1 | 89.49 (5) | N4—C13—H13 | 118.6 |
N2—Ni1—Cl1 | 166.31 (5) | C14—C13—H13 | 118.6 |
N3—Ni1—Cl2 | 87.94 (5) | C15—C14—C13 | 119.2 (2) |
N1—Ni1—Cl2 | 95.62 (6) | C15—C14—H14 | 120.4 |
N4—Ni1—Cl2 | 164.76 (5) | C13—C14—H14 | 120.4 |
N2—Ni1—Cl2 | 88.97 (5) | C14—C15—C16 | 119.0 (2) |
Cl1—Ni1—Cl2 | 93.97 (2) | C14—C15—H15 | 120.5 |
N1—O1—H1 | 109.5 | C16—C15—H15 | 120.5 |
N3—O2—H2 | 109.5 | C15—C16—C17 | 119.2 (2) |
C6—N1—O1 | 115.73 (17) | C15—C16—H16 | 120.4 |
C6—N1—Ni1 | 120.35 (15) | C17—C16—H16 | 120.4 |
O1—N1—Ni1 | 123.85 (12) | N4—C17—C16 | 121.86 (19) |
C1—N2—C5 | 118.66 (19) | N4—C17—C18 | 115.20 (18) |
C1—N2—Ni1 | 127.91 (16) | C16—C17—C18 | 122.9 (2) |
C5—N2—Ni1 | 113.37 (14) | N3—C18—C19 | 125.41 (19) |
C18—N3—O2 | 116.43 (18) | N3—C18—C17 | 112.33 (19) |
C18—N3—Ni1 | 120.22 (14) | C19—C18—C17 | 122.25 (18) |
O2—N3—Ni1 | 122.03 (13) | C20—C19—C24 | 118.9 (2) |
C13—N4—C17 | 117.97 (18) | C20—C19—C18 | 120.0 (2) |
C13—N4—Ni1 | 127.23 (15) | C24—C19—C18 | 121.1 (2) |
C17—N4—Ni1 | 114.43 (13) | C19—C20—C21 | 120.2 (2) |
N2—C1—C2 | 123.1 (2) | C19—C20—H20 | 119.9 |
N2—C1—H1A | 118.4 | C21—C20—H20 | 119.9 |
C2—C1—H1A | 118.4 | C22—C21—C20 | 120.2 (3) |
C3—C2—C1 | 118.1 (2) | C22—C21—H21 | 119.9 |
C3—C2—H2A | 121.0 | C20—C21—H21 | 119.9 |
C1—C2—H2A | 121.0 | C23—C22—C21 | 120.4 (3) |
C2—C3—C4 | 120.1 (2) | C23—C22—H22 | 119.8 |
C2—C3—H3 | 119.9 | C21—C22—H22 | 119.8 |
C4—C3—H3 | 119.9 | C22—C23—C24 | 120.1 (3) |
C3—C4—C5 | 118.7 (2) | C22—C23—H23 | 119.9 |
C3—C4—H4 | 120.6 | C24—C23—H23 | 119.9 |
C5—C4—H4 | 120.6 | C23—C24—C19 | 120.2 (2) |
N2—C5—C4 | 121.2 (2) | C23—C24—H24 | 119.9 |
N2—C5—C6 | 116.14 (18) | C19—C24—H24 | 119.9 |
C4—C5—C6 | 122.6 (2) | C26—C25—H25A | 109.5 |
N1—C6—C7 | 125.2 (2) | C26—C25—H25B | 109.5 |
N1—C6—C5 | 113.03 (19) | H25A—C25—H25B | 109.5 |
C7—C6—C5 | 121.78 (18) | C26—C25—H25C | 109.5 |
C12—C7—C8 | 119.1 (2) | H25A—C25—H25C | 109.5 |
C12—C7—C6 | 120.7 (2) | H25B—C25—H25C | 109.5 |
C8—C7—C6 | 120.2 (2) | O3—C26—C25 | 123.1 (3) |
C9—C8—C7 | 119.8 (3) | O3—C26—C27 | 122.5 (3) |
C9—C8—H8 | 120.1 | C25—C26—C27 | 114.4 (3) |
C7—C8—H8 | 120.1 | C26—C27—H27A | 109.5 |
C8—C9—C10 | 120.7 (3) | C26—C27—H27B | 109.5 |
C8—C9—H9 | 119.7 | H27A—C27—H27B | 109.5 |
C10—C9—H9 | 119.7 | C26—C27—H27C | 109.5 |
C11—C10—C9 | 119.7 (3) | H27A—C27—H27C | 109.5 |
C11—C10—H10 | 120.1 | H27B—C27—H27C | 109.5 |
N3—Ni1—N1—C6 | 26.9 (5) | O1—N1—C6—C7 | 0.3 (3) |
N4—Ni1—N1—C6 | 92.66 (17) | Ni1—N1—C6—C7 | 177.24 (16) |
N2—Ni1—N1—C6 | 3.62 (17) | O1—N1—C6—C5 | −179.56 (17) |
Cl1—Ni1—N1—C6 | −177.94 (17) | Ni1—N1—C6—C5 | −2.7 (3) |
Cl2—Ni1—N1—C6 | −84.00 (17) | N2—C5—C6—N1 | −0.9 (3) |
N3—Ni1—N1—O1 | −156.4 (4) | C4—C5—C6—N1 | 179.0 (2) |
N4—Ni1—N1—O1 | −90.70 (17) | N2—C5—C6—C7 | 179.2 (2) |
N2—Ni1—N1—O1 | −179.74 (18) | C4—C5—C6—C7 | −0.9 (3) |
Cl1—Ni1—N1—O1 | −1.30 (16) | N1—C6—C7—C12 | −121.8 (3) |
Cl2—Ni1—N1—O1 | 92.64 (16) | C5—C6—C7—C12 | 58.1 (3) |
N3—Ni1—N2—C1 | 3.12 (19) | N1—C6—C7—C8 | 58.4 (3) |
N1—Ni1—N2—C1 | 179.2 (2) | C5—C6—C7—C8 | −121.7 (2) |
N4—Ni1—N2—C1 | 80.01 (19) | C12—C7—C8—C9 | 0.2 (4) |
Cl1—Ni1—N2—C1 | 172.62 (17) | C6—C7—C8—C9 | −179.9 (2) |
Cl2—Ni1—N2—C1 | −84.74 (18) | C7—C8—C9—C10 | −0.4 (5) |
N3—Ni1—N2—C5 | −179.93 (15) | C8—C9—C10—C11 | 0.6 (5) |
N1—Ni1—N2—C5 | −3.81 (14) | C9—C10—C11—C12 | −0.5 (5) |
N4—Ni1—N2—C5 | −103.04 (15) | C10—C11—C12—C7 | 0.3 (4) |
Cl1—Ni1—N2—C5 | −10.4 (3) | C8—C7—C12—C11 | −0.2 (4) |
Cl2—Ni1—N2—C5 | 92.21 (14) | C6—C7—C12—C11 | −180.0 (2) |
N1—Ni1—N3—C18 | 59.8 (5) | C17—N4—C13—C14 | 0.4 (3) |
N4—Ni1—N3—C18 | −7.67 (16) | Ni1—N4—C13—C14 | 172.90 (16) |
N2—Ni1—N3—C18 | 82.58 (17) | N4—C13—C14—C15 | 0.3 (3) |
Cl1—Ni1—N3—C18 | −94.92 (16) | C13—C14—C15—C16 | −0.4 (3) |
Cl2—Ni1—N3—C18 | 171.40 (16) | C14—C15—C16—C17 | −0.1 (3) |
N1—Ni1—N3—O2 | −106.6 (4) | C13—N4—C17—C16 | −0.9 (3) |
N4—Ni1—N3—O2 | −174.12 (17) | Ni1—N4—C17—C16 | −174.40 (16) |
N2—Ni1—N3—O2 | −83.87 (16) | C13—N4—C17—C18 | 177.00 (17) |
Cl1—Ni1—N3—O2 | 98.64 (15) | Ni1—N4—C17—C18 | 3.5 (2) |
Cl2—Ni1—N3—O2 | 4.95 (15) | C15—C16—C17—N4 | 0.8 (3) |
N3—Ni1—N4—C13 | −171.15 (18) | C15—C16—C17—C18 | −176.94 (19) |
N1—Ni1—N4—C13 | 18.03 (18) | O2—N3—C18—C19 | −0.9 (3) |
N2—Ni1—N4—C13 | 94.97 (17) | Ni1—N3—C18—C19 | −168.04 (16) |
Cl1—Ni1—N4—C13 | −71.35 (16) | O2—N3—C18—C17 | 178.61 (16) |
Cl2—Ni1—N4—C13 | −174.69 (13) | Ni1—N3—C18—C17 | 11.4 (2) |
N3—Ni1—N4—C17 | 1.61 (13) | N4—C17—C18—N3 | −9.5 (3) |
N1—Ni1—N4—C17 | −169.20 (13) | C16—C17—C18—N3 | 168.4 (2) |
N2—Ni1—N4—C17 | −92.26 (14) | N4—C17—C18—C19 | 170.02 (18) |
Cl1—Ni1—N4—C17 | 101.42 (13) | C16—C17—C18—C19 | −12.1 (3) |
Cl2—Ni1—N4—C17 | −1.9 (3) | N3—C18—C19—C20 | 127.1 (3) |
C5—N2—C1—C2 | −1.4 (3) | C17—C18—C19—C20 | −52.4 (3) |
Ni1—N2—C1—C2 | 175.42 (19) | N3—C18—C19—C24 | −51.9 (3) |
N2—C1—C2—C3 | 0.2 (4) | C17—C18—C19—C24 | 128.6 (2) |
C1—C2—C3—C4 | 1.3 (4) | C24—C19—C20—C21 | 1.3 (4) |
C2—C3—C4—C5 | −1.6 (4) | C18—C19—C20—C21 | −177.7 (2) |
C1—N2—C5—C4 | 1.1 (3) | C19—C20—C21—C22 | −0.2 (4) |
Ni1—N2—C5—C4 | −176.19 (18) | C20—C21—C22—C23 | −0.9 (4) |
C1—N2—C5—C6 | −178.99 (19) | C21—C22—C23—C24 | 0.8 (4) |
Ni1—N2—C5—C6 | 3.7 (2) | C22—C23—C24—C19 | 0.3 (4) |
C3—C4—C5—N2 | 0.4 (4) | C20—C19—C24—C23 | −1.4 (4) |
C3—C4—C5—C6 | −179.5 (2) | C18—C19—C24—C23 | 177.6 (2) |