| Bruker APEXII CCD diffractometer | 1589 independent reflections |
| Radiation source: fine-focus sealed tube | 1048 reflections with I > 2σ(I) |
| graphite | Rint = 0.048 |
| φ and ω scans | θmax = 28.4°, θmin = 1.5° |
| Absorption correction: multi-scan (SADABS; Bruker, 2007) | h = −7→8 |
| Tmin = 0.976, Tmax = 0.995 | k = −9→9 |
| 5950 measured reflections | l = −22→35 |