| Refinement on F2 | 1 restraint |
| Least-squares matrix: full | H atoms treated by a mixture of independent and constrained refinement |
| R[F2 > 2σ(F2)] = 0.035 | w = 1/[σ2(Fo2) + (0.0573P)2] where P = (Fo2 + 2Fc2)/3 |
| wR(F2) = 0.099 | (Δ/σ)max = 0.001 |
| S = 1.05 | Δρmax = 0.23 e Å−3 |
| 2787 reflections | Δρmin = −0.21 e Å−3 |
| 220 parameters |